Publication Type |
Journal Article |
Title |
Structural characterisation of flavonoids and flavonoid-O-glycosides extracted from Genista tenera by fast-atom bombardment tandem mass spectrometry |
Authors |
Carlos M. Borges P Martinho Alice Martins Amélia P. Rauter MAA Ferreira |
Groups |
HC |
Journal |
RAPID COMMUNICATIONS IN MASS SPECTROMETRY |
Year |
2001 |
Month |
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|
Volume |
15 |
Number |
18 |
Pages |
1760-1767 |
Abstract |
Genista tenera is a plant native to the Madeira Island (Portugal). From the ethanol extract of its powdered aerial parts, two flavones, three isoflavones and one 7-O-glacosyl isoflavone were isolated. A mass spectrometric study of these compounds was performed using liquid secondary ion mass spectrometry (LSIMS) in combination with high-energy collision-induced dissociation (CID) and tandem mass spectrometry (MS/MS). Characteristic fragmentation patterns were observed in all the investigated compounds; the loss of small neutral species from the protonated molecules was useful for identifying the presence of specific functional groups in the A- and B-rings. In order to help to establish the proposed structures, NMR and UV studies were also performed. Copyright (C) 2001 John Wiley \& Sons, Ltd. |
DOI |
http://dx.doi.org/10.1002/rcm.436 |
ISBN |
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Publisher |
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Book Title |
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ISSN |
0951-4198 |
EISSN |
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Conference Name |
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Bibtex ID |
ISI:000171017900016 |
Observations |
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