Publication Type Journal Article
Title Liquid chromatography-diode array detection-electrospray ionisation mass spectrometry/nuclear magnetic resonance analyses of the anti-hyperglycemic flavonoid extract of Genista tenera - Structure elucidation of a flavonoid-C-glycoside
Authors Amélia P. Rauter Alice Martins Carlos M. Borges J Ferreira J Justino MR Bronze Ana V. Coelho YH Choi R Verpoorte
Groups HC
Journal JOURNAL OF CHROMATOGRAPHY A
Year 2005
Month September
Volume 1089
Number 1
Pages 59-64
Abstract The anti-hyperglycemic flavonoid extract obtained from Genista tenera was first studied by liquid chromatography (LC)-diode array detection (DAD) which showed the presence of two major compounds. One of them was identified as genistein-7-O-glucoside. Luteolin-7-O-glucoside was detected as a minor constituent, while luteolin-7,3 -di-O-glucoside and rutin were found in trace amounts. LC-DAD-ESI-MS and NMR were used to confirm the structure of these compounds and allowed the elucidation of the structure of the unknown major compound, which is the flavonoid 5,7,4 -trihydroxyisoflavone-8-C-glucoside. (c) 2005 Elsevier B.V. All rights reserved.
DOI http://dx.doi.org/10.1016/j.chroma.2005.06.046
ISBN
Publisher
Book Title
ISSN 0021-9673
EISSN
Conference Name
Bibtex ID ISI:000231200700008
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