Publication Type |
Journal Article |
Title |
Liquid chromatography-diode array detection-electrospray ionisation mass spectrometry/nuclear magnetic resonance analyses of the anti-hyperglycemic flavonoid extract of Genista tenera - Structure elucidation of a flavonoid-C-glycoside |
Authors |
Amélia P. Rauter Alice Martins Carlos M. Borges J Ferreira J Justino MR Bronze Ana V. Coelho YH Choi R Verpoorte |
Groups |
HC |
Journal |
JOURNAL OF CHROMATOGRAPHY A |
Year |
2005 |
Month |
September |
Volume |
1089 |
Number |
1 |
Pages |
59-64 |
Abstract |
The anti-hyperglycemic flavonoid extract obtained from Genista tenera was first studied by liquid chromatography (LC)-diode array detection (DAD) which showed the presence of two major compounds. One of them was identified as genistein-7-O-glucoside. Luteolin-7-O-glucoside was detected as a minor constituent, while luteolin-7,3 -di-O-glucoside and rutin were found in trace amounts. LC-DAD-ESI-MS and NMR were used to confirm the structure of these compounds and allowed the elucidation of the structure of the unknown major compound, which is the flavonoid 5,7,4 -trihydroxyisoflavone-8-C-glucoside. (c) 2005 Elsevier B.V. All rights reserved. |
DOI |
http://dx.doi.org/10.1016/j.chroma.2005.06.046 |
ISBN |
|
Publisher |
|
Book Title |
|
ISSN |
0021-9673 |
EISSN |
|
Conference Name |
|
Bibtex ID |
ISI:000231200700008 |
Observations |
|