Publication Type Journal Article
Title Comparison of pennyroyal oils obtained by supercritical CO2 extraction and hydrodistillation
Authors EMC Reis-Vasco José Coelho António Palavra
Groups MET
Journal FLAVOUR AND FRAGRANCE JOURNAL
Year 1999
Month May
Volume 14
Number 3
Pages 156-160
Abstract Flowers and leaves of pennyroyal (Mentha pulegium L.) were extracted using supercritical CO2 followed by a two-stage fractional separation technique. Using a flow apparatus with an extraction vessel (11) and two separators (0.271), the best conditions of extraction (P = 100 bar and T = 50 degrees C) and of separation (P = 80 bar, T = -16 degrees C for the first separator and P = 18 bar, T = 0 degrees C for the second) were found and used to investigate the effect of different mean particle diameters. The pennyroyal oil obtained under these conditions was compared with that obtained by hydrodistillation. Twenty-one components were identified by GC-MS and quantified by GC. Both the hydrodistillation and supercritical oils of Mentha pulegium L. contain the oxygenated monoterpenes pulegone (approximate to 80\%) and menthone (approximate to 9\%) as the main components. The aroma of the pennyroyal oil obtained with supercritical CO2 was closer to that of the starting vegetable material than the aroma of the essential oil produced by hydrodistillation. Copyright (C) 1999 John Wiley \& Sons, Ltd.
DOI http://dx.doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<156::AID-FFJ793>3.0.CO;2-J
ISBN
Publisher WILEY-BLACKWELL
Book Title
ISSN 0882-5734
EISSN
Conference Name
Bibtex ID ISI:000080789700002
Observations
Back to Publications List