| Publication Type |
Journal Article |
| Title |
Kinetic parameters of thermal decomposition of rare earth perchlorates complexes with lactame |
| Authors |
AMG Pedrosa Mary K. S. Batista FMM Borges LB Zinner HS Scatena DM Melo |
| Groups |
|
| Journal |
ECLETICA QUIMICA |
| Year |
2002 |
| Month |
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|
| Volume |
27 |
| Number |
|
| Pages |
31-40 |
| Abstract |
Complexes of rare earth perchlorates with 2-azacyclononanone (AZA) were synthesized (molar ratio 1:8) by reaction of hydrated perchlorates in ethanol and triethlylorthoformate by a vapor diffusion method and they were characterized by complexometric analyses with EDTA, CHN microanalytical procedures, IR absorption spectra, thermogravimetry in air and N(2) atmosphere and differential scanning calorimetry (DSC) in the N(2) atmosphere. The theoretical kinetic study was carried out using the OBASIC program inputting the TG data. |
| DOI |
http://dx.doi.org/ |
| ISBN |
|
| Publisher |
|
| Book Title |
|
| ISSN |
0100-4670 |
| EISSN |
|
| Conference Name |
|
| Bibtex ID |
ISI:000179435100003 |
| Observations |
|
